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Pharm Sci. 2023;29(2): 208-218.
doi: 10.34172/PS.2022.34

Scopus ID: 85150181955
  Abstract View: 662
  PDF Download: 573

Research Article

Preparation and In-Vitro Evaluation of Ketoconazole-Loaded Niosome (Ketosome) for Drug Delivery to Cutaneous Candidiasis

Katayoun Morteza-Semnani 1 ORCID logo, Majid Saeedi 2,3 ORCID logo, Jafar Akbari 3, Maryam Moazeni 4,5, Amirhossein Babaei 3,6 ORCID logo, Reza Negarandeh 3,6, Maedeh Azizi 6, Mohammad Eghbali 2,3, Seyyed Mohammad Hassan Hashemi 7* ORCID logo

1 Department of Medicinal Chemistry, Faculty of Pharmacy, Mazandaran University of Medical Sciences, Sari, Iran.
2 Pharmaceutical Sciences Research Centre, Haemoglobinopathy Institute, Mazandaran University of Medical Sciences, Sari, Iran.
3 Department of Pharmaceutics, Faculty of Pharmacy, Mazandaran University of Medical Sciences, Sari, Iran.
4 Department of Medical Mycology and Parasitology, Faculty of Medicine, Mazandaran University of Medical Sciences, Sari, Iran.
5 Invasive Fungi Research Centre, Communicable Disease Institute, Mazandaran University of Medical Sciences, Sari, Iran.
6 Student Research Committee Center, Mazandaran University of Medical Sciences, Sari, Iran.
7 Department of Pharmaceutics, Faculty of Pharmacy, Hormozgan University of Medical Sciences, Bandar Abbas, Iran.
*Corresponding Author: Email: smhhashemipharma@gmail.com

Abstract

Background: Recently, niosomes are becoming popular in drug delivery. The current work aimed to investigate the characteristics, cellular safety, and antifungal activity of ketoconazole-loaded niosome (ketosome).

Methods: Ultrasonic approach was employed to prepare ketosome including cholesterol, nonionic surfactant and ketoconazole. The size characteristics and morphological features of ketosome and physicochemical properties of ketoconazole in ketosomes were evaluated using dynamic light scattering (DLS), differential scanning calorimetry (DSC), powder x-ray diffractometer (PXRD), scanning electron microscopy (SEM), and attenuated total reflectance-Fourier transform infrared (ATR-FTIR) spectroscopy. Also, the dissolution rate, cellular safety test and antimycotic properties of ketosome were examined.

Results: According to the results, the particle size of the ketosome decreased from 491.400±10.622 to 121.300±7.274 nm by the increment of cholesterol. According to further research, changes in the cholesterol:surfactants ratio can modulate the zeta potential from -27.866±1.069 to -12.500±1.153 mV. The highest entrapment of ketoconazole was about 87% when the cholesterol concentration in the ketosome was high. Ketosome with the maximum cholesterol:surfactants ratio showed the fastest drug release. Furthermore, the cell viability assay revealed that the ketosome had lower cytotoxicity in comparison with pure drug. The cell viability of the ketosome was estimated to be about 90% (HGF cell line). The ketosome had a lower MIC than the pure drug when tested against Candida albicans.

Conclusion: The results of this study revealed that the optimized ketoconazole-loaded niosome could be used as a possible nanovesicle for ketoconazole drug delivery, potentially opening up new ways for the management of cutaneous candidiasis complaints.

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Submitted: 09 Apr 2022
Revision: 15 Jul 2022
Accepted: 16 Jul 2022
ePublished: 22 Jul 2022
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